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  • Application of a chiral metal-organic framework in enantioselective separation.

Application of a chiral metal-organic framework in enantioselective separation.

Chemical communications (Cambridge, England) (2011-10-01)
Mohan Padmanaban, Philipp Müller, Christian Lieder, Kristina Gedrich, Ronny Grünker, Volodymyr Bon, Irena Senkovska, Sandra Baumgärtner, Sabine Opelt, Silvia Paasch, Eike Brunner, Frank Glorius, Elias Klemm, Stefan Kaskel
ABSTRACT

A modular approach for the synthesis of highly ordered porous and chiral auxiliary (Evans auxiliary) decorated metal-organic frameworks is developed. Our synthesis strategy, which uses known porous structures as model materials for incorporation of chirality via linker modification, can provide access to a wide range of porous materials suitable for enantioselective separation and catalysis. Chiral analogues of UMCM-1 have been synthesized and investigated for the enantioseparation of chiral compounds in the liquid phase and first promising results are reported.

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
1-Phenylethanol, 98%
Sigma-Aldrich
α-Methylbenzyl alcohol, ≥99%, FCC, FG