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  • Versatile synthesis of end-reactive polyrotaxanes applicable to fabrication of supramolecular biomaterials.

Versatile synthesis of end-reactive polyrotaxanes applicable to fabrication of supramolecular biomaterials.

Beilstein journal of organic chemistry (2017-02-02)
Atsushi Tamura, Asato Tonegawa, Yoshinori Arisaka, Nobuhiko Yui
ABSTRACT

Cyclodextrin (CD)-threaded polyrotaxanes (PRXs) with reactive functional groups at the terminals of the axle polymers are attractive candidates for the design of supramolecular materials. Herein, we describe a novel and simple synthetic method for end-reactive PRXs using bis(2-amino-3-phenylpropyl) poly(ethylene glycol) (PEG-Ph-NH

MATERIALS
Product Number
Brand
Product Description

Sigma-Aldrich
4-Azidobenzoic acid solution, ~0.2 M in tert-butyl methyl ether, ≥95.0% (HPLC)
Sigma-Aldrich
4-tert-Butylphenylacetylene, 96%