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CRM69151

Supelco

Chlorobenzilate

certified reference material, TraceCERT®, Manufactured by: Sigma-Aldrich Production GmbH, Switzerland

Synonym(s):

Ethyl 4,4′-dichlorobenzilate

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About This Item

Empirical Formula (Hill Notation):
C16H14Cl2O3
CAS Number:
510-15-6
Molecular Weight:
325.19
MDL number:
MFCD00055312
UNSPSC Code:
41116107
NACRES:
NA.24

grade

certified reference material
TraceCERT®

Quality Level

300

product line

TraceCERT®

shelf life

limited shelf life, expiry date on the label

manufacturer/tradename

Manufactured by: Sigma-Aldrich Production GmbH, Switzerland

format

neat

storage temp.

2-8°C

SMILES string

CCOC(=O)C(O)(c1ccc(Cl)cc1)c2ccc(Cl)cc2

InChI

1S/C16H14Cl2O3/c1-2-21-15(19)16(20,11-3-7-13(17)8-4-11)12-5-9-14(18)10-6-12/h3-10,20H,2H2,1H3

InChI key

RAPBNVDSDCTNRC-UHFFFAOYSA-N

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General description

This certified reference material (CRM) is produced and certified in accordance with ISO/IEC 17025 and ISO 17034. This CRM is traceable to primary material from an NMI, e.g. NIST or NMIJ.
Certified content by quantitative NMR incl. uncertainty and expiry date are given on the certificate.
Download your certificate at: http://www.sigma-aldrich.com

Chlorobenzilate is a non-systemic acaricide, used for the control of mites in pome fruit, citrus, vines, soybeans, cotton, tea, vegetables, and beehives.
Chlorobenzilate is not approved for use as a plant protection product in the European Union (EU) as per the Commission Regulation 1107/2009.

Application

The certified reference material (CRM) is intended to be used as a calibrant for chromatography and other analytical techniques.
Chlorobenzilate CRM may also be used as given below:

  • Quantification of 72 pesticide residues in 35 different fruit and vegetable samples using microwave-assisted extraction (MAE) accompanied by dispersive solid-phase extraction (d-SPE) and separation plus detection by retention time locked (RTL) capillary gas-chromatography and mass spectrometry (MS) respectively
  • Multi-residue analysis of 35 pesticides from various chemical classes melon samples by QuEChERS based sample preparation and determination by gas chromatography-single quadrupole mass spectrometry (GC-SQ/MS)
  • Monitoring of 86 pesticides in 13 different samples of non-leafy vegetables by gas chromatography with mass spectrometric detection (GC-MS)
  • Evaluate a multi-residue method based on gas chromatography-triple quadrupole mass spectrometry (GC-QqQMS/MS) for the analysis of 203 pesticides in 69 fruit and vegetable samples for a shorter runtime
  • Simultaneous determination of 124 pesticide residues in rice samples by using dispersive solid-phase extraction (d-SPE) for sample clean-up and gas chromatography-tandem mass spectrometry (GC-MS/MS) for detection
  • Analysis of 113 pesticide residues and their metabolites in a broad range of fruit and vegetables representing high water and high acid content matrices by a deactivated PTV (programmable temperature vaporizing) injector liner and GC-MS/MS

Recommended products

Find a digital Reference Material for this product available on our online platform ChemisTwin® for NMR. You can use this digital equivalent on ChemisTwin® for your sample identity confirmation and compound quantification (with digital external standard). An NMR spectrum of this substance can be viewed and an online comparison against your sample can be performed with a few mouseclicks. Learn more here and start your free trial.

Legal Information

TraceCERT is a registered trademark of Merck KGaA, Darmstadt, Germany

pictograms

Exclamation markEnvironment
GHS07,GHS09

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Warning

Hazard Classifications

Acute Tox. 4 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Eye Irrit. 2

wgk_germany

WGK 3

flash_point_f

Not applicable

flash_point_c

Not applicable

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Certificates of Analysis (COA)

Lot/Batch Number
BCCF3057

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Xue Hou et al.
Food chemistry, 138(2-3), 1198-1205 (2013-02-16)
A modified QuEChERS method for simultaneous determination of 124 pesticide residues in rice was established and validated. The rice samples were initially extracted with acetonitrile (MeCN), and the targeted pesticides were purified following the dispersive solid phase extraction (d-SPE) cleanup

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